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Biomonitoring Quality Assurance Support Program |
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Analytical Method Report |
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Environmental Phenols |
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Laboratory Information |
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1 |
State Report: |
Select State |
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2 |
Results for Method: |
Select Method |
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Sample Preparation Information: |
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3 |
Does your method use automation: |
Yes or No |
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4 |
Does your sample preparation method include: |
Select SPE |
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5 |
Solid phase extraction platform: |
N/A |
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Additional information on sample prep procedure: |
Type description here |
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6 |
What is the method sample volume size: |
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7 |
Name of enzyme: |
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Enzyme Vendor |
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Enzyme Concentration |
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(please include units) |
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Amount |
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How long do you incubate the samples |
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Temperature during incubations |
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Degrees Celsius |
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HPLC Configuration: |
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8 |
Instrument manufacturer |
Select |
Type Other Here |
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9 |
What is the flow rate: |
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10 |
What is the method run time: |
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11 |
What is the sample injection volume: |
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12 |
Column name and Manufacturer |
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13 |
Column dimensions |
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14 |
Elution Type: |
Select |
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15 |
Mobile Phase A Composition |
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Describe composition for Mobile Phase A |
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16 |
Mobile Phase B Composition |
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Describe composition for Mobile Phase B |
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Mass Spectrometer Configuration |
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17 |
Have you optimized the MS Parameters for your method? (Analytes, Precursor and Product Ions, Collision Energy) |
Yes or No |
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18 |
What is the ionization mode: |
Select Mode |
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20 |
Please complete the table for each analytes LOD, precursor and product ion transitions: |
Analyte |
LOD |
Calibration Range |
Precursor Ion (mass) |
Product Ion (mass) |
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Example: MCPP |
0.4 ng/ml |
0.035 - 350 ng/ml |
251 |
103 |
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13C4-MCPP |
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225 |
103 |
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Analytical and Internal Standards |
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Please complete the table for metabolite standards: |
Analytical and Internal Standard |
Vendor |
Purity |
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Phthalate Metabolites |
Cambridge Isotope Laboratory |
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25 |
How do you prepare your standards? |
Select |
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27 |
How many points are in the calibration curve? |
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28 |
Is the calibration curve weighted? |
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weighted curve: No weighting, 1/X, 1/X^2,Other ? |
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29 |
What integration software do you use? |
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Additional Method Questions |
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30 |
Which proficiency testing programs do you participate in? |
Select |
Please type other programs here |
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31 |
what is the average number of samples analyzed per month for this method? |
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32 |
Have you checked the accuracy of the method using NIST SRMs? |
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33 |
What volume of sample is required for BQASP Analysis? |
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Please provide a screenshot of your results chromatography: |
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