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Biomonitoring Quality Assurance Support Program |
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Analytical Method Report |
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UNIVERSAL PESTICIDES |
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Laboratory Information |
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1 |
State Report: |
Select State |
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2 |
Results for Method: |
Select Method |
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Sample Preparation Information: |
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3 |
Does your method use automation: |
Yes or No |
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4 |
Does your sample preparation method include: |
Select SPE |
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5 |
Solid phase extraction platform: |
N/A |
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Additional information on sample prep procedure: |
Type description here |
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6 |
What is the method sample volume size: |
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7 |
Name of enzyme: |
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Enzyme Vendor |
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Enzyme Concentration |
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(please include units) |
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Amount |
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How long do you incubate the samples |
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Temperature during incubations |
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Degrees Celsius |
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HPLC Configuration: |
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8 |
Instrument manufacturer |
Select |
Type Other Here |
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9 |
What is the flow rate: |
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10 |
What is the method run time: |
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11 |
What is the sample injection volume: |
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12 |
Column name and Manufacturer |
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13 |
Column dimensions |
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14 |
Elution Type: |
Select |
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15 |
Mobile Phase A Composition |
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Describe composition for Mobile Phase A |
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16 |
Mobile Phase B Composition |
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Describe composition for Mobile Phase B |
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Mass Spectrometer Configuration |
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17 |
Have you optimized the MS Parameters for your method? (Analytes, Precursor and Product Ions, Collision Energy) |
Yes or No |
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18 |
What is the ionization mode: |
Select Mode |
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20 |
Please complete the table for each analytes LOD, precursor and product ion transitions: |
Analyte |
LOD |
Calibration Range |
Precursor Ion (mass) |
Product Ion (mass) |
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Example: MCPP |
0.4 ng/ml |
0.035 - 350 ng/ml |
251 |
103 |
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13C4-MCPP |
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225 |
103 |
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Analytical and Internal Standards |
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Please complete the table for metabolite standards: |
Analytical and Internal Standard |
Vendor |
Purity |
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Phthalate Metabolites |
Cambridge Isotope Laboratory |
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25 |
How do you prepare your standards? |
Select |
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27 |
How many points are in the calibration curve? |
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28 |
Is the calibration curve weighted? |
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weighted curve: No weighting, 1/X, 1/X^2,Other ? |
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29 |
What integration software do you use? |
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Additional Method Questions |
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30 |
Which proficiency testing programs do you participate in? |
Select |
Please type other programs here |
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31 |
what is the average number of samples analyzed per month for this method? |
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32 |
Have you checked the accuracy of the method using NIST SRMs? |
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33 |
What volume of sample is required for BQASP Analysis? |
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Please provide a screenshot of your results chromatography: |
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UNIVERSAL PESTICIDES |
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PT Event ID: |
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Participant: |
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Analyst: |
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Reviewer: |
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Units of Result: |
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Sample ID |
Analyte |
Reported Value |
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20190F001UPSU |
3,5,6-trichloro-2-pyridinol |
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20190F001UPSU |
3-phenoxybenzoic acid |
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20190F001UPSU |
2-Isopropyl-4-methyl-6-hydroxypyrimidine |
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20190F001UPSU |
3-ph2-diethylamino-6-methyl pyrimidin-4-olenoxybenzoic acid |
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20190F001UPSU |
Malathion dicarboxylic acid |
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20190F001UPSU |
Trans-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropane-1- carboxylic acid |
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20190F001UPSU |
Cis-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropane-1- carboxylic acid |
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20190F001UPSU |
4-fluoro-3-phenoxy-benzoic acid |
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20190F001UPSU |
Para-nitrophenol |
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20190F001UPSU |
2,4-dichlorophenoxyacetic acid |
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Sample ID |
Analyte |
Reported Value |
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20190F002UPSU |
3,5,6-trichloro-2-pyridinol |
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20190F002UPSU |
3-phenoxybenzoic acid |
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20190F002UPSU |
2-Isopropyl-4-methyl-6-hydroxypyrimidine |
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20190F002UPSU |
3-ph2-diethylamino-6-methyl pyrimidin-4-olenoxybenzoic acid |
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20190F002UPSU |
Malathion dicarboxylic acid |
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20190F002UPSU |
Trans-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropane-1- carboxylic acid |
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20190F002UPSU |
Cis-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropane-1- carboxylic acid |
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20190F002UPSU |
4-fluoro-3-phenoxy-benzoic acid |
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20190F002UPSU |
Para-nitrophenol |
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20190F002UPSU |
2,4-dichlorophenoxyacetic acid |
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By submitting this form, we attest that the results reported were produced in this laboratory from the analysis of proficiency testing samples that were introduced into the routine workflow of the laboratory and analyzed using protocols and procedures with the same frequency routinely applied to patient specimens.
We further attest that the laboratory did not discuss or engage in any communications with anyone outside of our laboratory regarding the proficiency test or the results obtained. |
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